Idemitsu Kosan has patented a method for producing a sulfide solid electrolyte with an argyrodite crystal structure. The process involves mixing a raw material with elemental phosphorus at a specific power level and heat-treating the mixture within a defined temperature range. GlobalData’s report on Idemitsu Kosan gives a 360-degree view of the company including its patenting strategy. Buy the report here.
According to GlobalData’s company profile on Idemitsu Kosan, Anti-wear lubricants was a key innovation area identified from patents. Idemitsu Kosan's grant share as of February 2024 was 40%. Grant share is based on the ratio of number of grants to total number of patents.
Method for producing sulfide solid electrolyte with argyrodite crystal structure
A recently granted patent (Publication Number: US11916191B2) discloses a method for producing a sulfide solid electrolyte with an argyrodite crystal structure. The method involves mixing a raw material containing elemental phosphorus at a specific integrated power level and heat-treating the resulting precursor within a temperature range of 350 to 500°C. The integrated power during mixing is crucial, falling within the range of 0.5 to 20 kWh/kg, with further optional raw materials including elemental sulfur, lithium, chlorine, and/or bromine. The precursor obtained may contain P2S64- glass, with specific peak intensity requirements in solid 31P-NMR measurements to ensure quality.
Additionally, the patent outlines specific parameters for the heat-treating process, emphasizing atmospheric pressure and an inert atmosphere. The temperature during heat treatment should be at least 360°C, preferably falling within the range of 380 to 450°C, and conducted for a duration of 0.5 to 12 hours. The weight loss ratio of the precursor at 600°C should not exceed 1.5%, with integrated power during mixing limited to 1 to 10 kWh/kg. Furthermore, the mixing time is specified to be between 10 minutes to 10 hours, ensuring the production of a sulfide solid electrolyte with the desired crystal structure and properties.
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